Gas chromatographic-mass spectrometric analysis of pyrolytic oil distillates, 1978

Selasie, Mulugeta Haile

1970-1979

A sample of pyrolytic oil (condenser oil project B-469) was vacuum distilled at 30C/14.5mm - 188C/19.0mm. The distillate (25-1) was studied by gas chromatography to establish optimum conditions and apparatus performance for the separation of the components of the distillate. This was achieved by using a 6' x 1/4" SE-30 column. The peaks were identified by using a combined gas chromatographic and mass spectrometric technique. The identification of peaks was also aided by noting enhancement of peak size when known materials were chromatographed with the mixture. After the components of the mixture were known, a quantitative gas chromatographic analysis procedure was developed.

text

application/pdf

1978-12-01

thesis

Master of Science (MS)

Atlanta University

Chemistry

Polk, Malcolm B.

Clark Atlanta University

Georgia--Atlanta

http://hdl.handle.net/20.500.12322/cau.td:1978_selasie_mulugeta_h